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Hi this is Dr. Hill. You would see signs within 30 -60 minutes. Signs would be panting, hyper excitability, sometimes nausea and diarrhea if large amount ingested. I would make sure that Cody is monitored through the day if possible and walked every few hours. You want him to drink water and evacuate his bladder so as not to reabsorb any caffeine from urine. Please post any follow up questions. If you are satisfied with my response, then please take time to rate my response. You can continue posting on this thread for a couple of days, even after rating my response.